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<title>UTas ePrints - Coordination Chemistry of dimethylgold(III) and Methylmercury(II). Synthesis, 'H N.M.R. and Structural Studies of Poly(pyrazol-1-y1)borate Complexes</title>
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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Minchin, N.J." name="eprints.creators_name" />
<meta content="Patrick, J.M." name="eprints.creators_name" />
<meta content="White, A.H." name="eprints.creators_name" />
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<meta content="Dimethylgold(111) and methylmercury(11) form complexes Me2AuL and MeHgL where L are poly(pyrazol-1-y1)borate ligands [HB(pz)3]- and [B(pz)4]-. The structure of Me2Au{HB(pz)3} has been determined by single-crystal X-ray diffraction at 295 K and refined by least-squares methods to R 0.056 for 2194 independent 'observed' reflections. This complex has square-planar coordination for the gold atom involving two coordinated pyrazole rings and one uncoordinated ring, in contrast to the isoelectronic cation [Me2Au{(pz)3CH)]+ which has square planar coordination with a weak axial Au . .N interaction. Variable temperature 'H n.m.r. spectra in CD2Cl2 indicate presence of rapid equilibria between pyrazole ring environments at ambient temperature and, for the MeHg(II_
complexes, down to -90°C. For the Me2Au(III) complexes spectra at -9OoC indicate presence of pyrazole ring environments in ratios 2:1 (L = [HB(pz)3]-) and 2:1:1 (L = [B(pz)4]-). Crystal data for Me2Au{HB(pz)3}: rhombohedral, space group R3c, a 17.98(1) A, alpha 117.98(5), Z 18." name="eprints.abstract" />
<meta content="1983" name="eprints.date" />
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' Canty, A. J., Minchin, N. J., Healy, P. C., and White, A. H., J. Chem. Soc., Dalton Trans., 1982,
1795.
Canty, A. J., Chaichit, N., Gatehouse, B. M., and George, E. E., Inorg. Chem., 1981, 20, 4293.
Brownlee, R. T. C., Canty, A. J., and Mackay, M. F., Aust. J. Chem., 1978, 31, 1933.
See, e.g., Trofimenko, S., J. Am. Chenz. Soc., 1967, 89, 3170.
Borkett, N. F., Bruce, M. I., and Walsh, J. D., Aust. J. Chem., 1980, 33, 949.
Rabenstein, D. L., Acc. Chem. Res., 1978, 11, 100.
Canty, A. J., and Tobias, R. S., Inorg. Chem., 1979, 18, 413." name="eprints.referencetext" />
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<meta content="Dimethylgold(111) and methylmercury(11) form complexes Me2AuL and MeHgL where L are poly(pyrazol-1-y1)borate ligands [HB(pz)3]- and [B(pz)4]-. The structure of Me2Au{HB(pz)3} has been determined by single-crystal X-ray diffraction at 295 K and refined by least-squares methods to R 0.056 for 2194 independent 'observed' reflections. This complex has square-planar coordination for the gold atom involving two coordinated pyrazole rings and one uncoordinated ring, in contrast to the isoelectronic cation [Me2Au{(pz)3CH)]+ which has square planar coordination with a weak axial Au . .N interaction. Variable temperature 'H n.m.r. spectra in CD2Cl2 indicate presence of rapid equilibria between pyrazole ring environments at ambient temperature and, for the MeHg(II_
complexes, down to -90°C. For the Me2Au(III) complexes spectra at -9OoC indicate presence of pyrazole ring environments in ratios 2:1 (L = [HB(pz)3]-) and 2:1:1 (L = [B(pz)4]-). Crystal data for Me2Au{HB(pz)3}: rhombohedral, space group R3c, a 17.98(1) A, alpha 117.98(5), Z 18." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Coordination Chemistry of dimethylgold(III) and Methylmercury(II). Synthesis, 'H N.M.R. and Structural Studies of Poly(pyrazol-1-y1)borate Complexes</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Minchin, N.J.</span> and <span class="person_name">Patrick, J.M.</span> and <span class="person_name">White, A.H.</span> (1983) <xhtml:em>Coordination Chemistry of dimethylgold(III) and Methylmercury(II). Synthesis, 'H N.M.R. and Structural Studies of Poly(pyrazol-1-y1)borate Complexes.</xhtml:em> Australian Journal of Chemistry, 36 (6). pp. 1107-1113. ISSN 0004-9425</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2824/1/AustJ1983_2C_1107.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" class="ep_doc_icon" border="0" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2824/1/AustJ1983_2C_1107.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />294Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input accept-charset="utf-8" value="4023" name="docid" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://www.publish.csiro.au/nid/51/paper/CH9831107.htm">http://www.publish.csiro.au/nid/51/paper/CH9831107.htm</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">Dimethylgold(111) and methylmercury(11) form complexes Me2AuL and MeHgL where L are poly(pyrazol-1-y1)borate ligands [HB(pz)3]- and [B(pz)4]-. The structure of Me2Au{HB(pz)3} has been determined by single-crystal X-ray diffraction at 295 K and refined by least-squares methods to R 0.056 for 2194 independent 'observed' reflections. This complex has square-planar coordination for the gold atom involving two coordinated pyrazole rings and one uncoordinated ring, in contrast to the isoelectronic cation [Me2Au{(pz)3CH)]+ which has square planar coordination with a weak axial Au . .N interaction. Variable temperature 'H n.m.r. spectra in CD2Cl2 indicate presence of rapid equilibria between pyrazole ring environments at ambient temperature and, for the MeHg(II_
complexes, down to -90°C. For the Me2Au(III) complexes spectra at -9OoC indicate presence of pyrazole ring environments in ratios 2:1 (L = [HB(pz)3]-) and 2:1:1 (L = [B(pz)4]-). Crystal data for Me2Au{HB(pz)3}: rhombohedral, space group R3c, a 17.98(1) A, alpha 117.98(5), Z 18.</p></div><table style="margin-bottom: 1em" cellpadding="3" class="not_ep_block" border="0"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/259901.html">250000 Chemical Sciences > 259900 Other Chemical Sciences > 259901 Organometallic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2824</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">11 Jan 2008 11:00</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">11 Jan 2008 11:00</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2824;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2824">item control page</a></p>
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